| 1 | Define and sample each lot Separate lots by crop, harvest period, origin, storage location, and processing status. | An unrepresentative sample can conceal localized mold, chemical residues, or contamination. | Use a documented sampling plan based on Codex CAC/GL 50-2004 principles. Collect incremental portions from multiple bags, bulk points, or loading sections and combine them into a representative composite sample. | Identify the lot size, sampling locations, number of increments, composite-sample weight, sampler, date, and seal number before testing. | Sampling plan Chain of custody Retained sample log |
| 2 | Screen for aflatoxins Give special attention to peanuts, maize-derived oilseeds, cottonseed, and lots exposed to heat and moisture. | Aflatoxin B1 and total aflatoxins are produced by certain Aspergillus molds and can be unevenly distributed within a lot. | Use a validated rapid screening method for segregation, followed by confirmatory HPLC with fluorescence detection or LC-MS/MS through a competent laboratory. | Release only when AFB1 and total aflatoxins comply with the importing country’s commodity-specific limits. For example, some regulated markets apply limits near 2 µg/kg for AFB1 and 4 µg/kg for total aflatoxins in certain foods; requirements vary by product and use. | Aflatoxin result Method and LOQ Laboratory accreditation |
| 3 | Check pesticide residues Verify crop-protection records before accepting the lot for export. | Residues may comply with the production-country rules but exceed the importing country’s maximum residue level (MRL). | Request a multi-residue analysis using validated GC-MS/MS and LC-MS/MS methods. Include pesticides authorized or historically used on the specific crop and region. | Compare every detected residue with the destination-market MRL. Where no MRL exists, buyers may apply the statutory default limit or a contractual limit; the report should show the result and laboratory LOQ. | Spray records Pre-harvest intervals Multi-residue report |
| 4 | Test for Salmonella Control contamination after harvest, during handling, and in shared processing equipment. | Raw oilseeds can carry pathogens even when they look clean and have normal moisture. | Use a recognized detection method such as ISO 6579-1, including pre-enrichment, selective enrichment, and confirmation. | A common buyer requirement for ready-to-eat or further-processed ingredients is not detected in 25 g. Confirm the exact requirement because legal criteria differ by destination, product category, and intended use. | Pathogen test report Sanitation records Corrective-action log |
| 5 | Dry and monitor moisture Cool the crop after drying and prevent condensation during storage and loading. | Excess moisture increases mold growth, heating, rancidity, caking, and insect activity. | Measure moisture with a calibrated instrument and verify periodically by a reference oven method appropriate to the commodity, such as ISO 665 for oilseeds. | Typical commercial targets vary: soybeans are often traded around 13% moisture, while sunflower seed is often around 8–9%. Use the signed contract specification and avoid storing warm or damp seed. | Moisture readings Dryer settings Temperature records |
| 6 | Remove foreign material and insects Clean, grade, and inspect before packing or bulk loading. | Stones, metal, plant debris, damaged kernels, live insects, and insect fragments can cause rejection or safety concerns. | Use sieving, aspiration, magnets or metal detection, visual inspection, and an insect check. Record damaged-kernel, foreign-material, and infestation results. | No live insects, rodent contamination, or visible mold. Foreign-material and damaged-kernel percentages must meet the buyer’s commodity specification because limits differ significantly among oilseeds. | Cleaning report Inspection checklist Pest-control records |
| 7 | Complete traceability and pre-shipment release Keep each tested lot physically and digitally identifiable through loading. | Mixing tested and untested material, damaged packaging, or contaminated containers can invalidate otherwise acceptable results. | Review the certificate of analysis, lot code, origin, harvest year, treatment declaration, packaging condition, container cleanliness, seal number, and test dates before dispatch. | Use a retained sample and release checklist. Results should be linked to the exact lot shipped, with sufficient remaining shelf life and transport conditions documented. | Certificate of analysis Traceability map Container inspection Shipping release form |